X-ray powder diffrac­tion (XRPD)

X-ray techniques | Material composition | Solid

Identification of crystalline phases, structural analysis, analysis of material properties

Description of the method

X-ray powder diffraction is used to identify crystalline phases, determine structure and analyse material properties. It is based on the diffraction of X-rays by the regularly arranged atoms in crystal lattices. To do this, the samples must be ground into a fine, homogeneous powder. 

Examples of applications

  • Phase identification and quantitative phase analysis
  • Analysis of phase changes under specific conditions such as temperature, humidity and applied pressure (non-ambient investigations)
  • Analysis of physical properties such as crystallite size, crystallite orientation and residual stress (‘microstructure’ of polycrystalline materials).
  • Quality control in the cement, ceramics and steel industries
  • Characterisation of new inorganic materials
  • Monitoring of hydration processes
  • Analysis of mineral compositions

Contact

Associate Professor Dr Gunther Heymann
Department of General and Inorganic and Theoretical Chemistry
Innrain 80–82, 6020 Innsbruck
 +43 (512) 507 57003
Email Website

  • Measurements at room temperature and at temperatures up to 1100 °C

Associate Professor Dr Thomas Lörting
Department of Physical Chemistry
Innrain 52c, 6020 Innsbruck
+43 (512) 507 58019
Email Website

  • Low-temperature XRPD

Professor Volker Kahlenberg
Institute of Mineralogy and Petrography
Innrain 52, 6020 Innsbruck
 +43 (512) 507 54603 
Email Website

  • Measurements also using mixtures of various inert/reactive gases such as He,CO₂,H₂, CO.
  • Qualitative and quantitative phase analysis of crystalline and amorphous phases
  • Extensive experience with a wide variety of industrial samples from the ceramics, binders, building materials, glass and waste materials sectors, such as slag and ores.
  • Analytical services for industrial partners in Austria and other European countries.

Prof. Dr Hubert Huppertz
Department of General, Inorganic and Theoretical Chemistry
Innrain 80–82, 6020 Innsbruck
 +43 (512) 507 57000
Email Website

  • High-temperature XRPD

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