Description of the method
Highly magnified view of surfaces. The following technologies are available:
Analyses in the micro- to nanometre range:
- Scanning electron microscopy (SEM): An electron beam scans the sample surface; the interaction provides high-resolution topographical and chemical information.
- Scanning transmission electron microscopy (STEM):Same operating principle as SEM, but the beam penetrates the (thin) sample and provides information about the internal structures.
Analyses at the atomic level:
- Scanning tunnelling microscopy (STM) and scanning tunnelling spectroscopy (STS): STM: At small distances (< 1 nm) between the conductive tip and the sample, a measurable tunnelling current flows, allowing individual atoms and their electronic properties to be visualised. RTS additionally provides electronic information about the density of states.
- Atomic force microscopy (AFM): A nanoscale-scale fine needle is pressed against the sample to be measured by means of a leaf spring, and the atomic forces cause the leaf spring to bend. Unlike STM, non-conductive samples can also be analysed.
- Atomic force microscopy with IR coupling (AFM-IR):This hybrid technique combines the high spatial resolution of AFM with the chemical specificity of IR spectroscopy. The IR-induced thermal expansion of the sample is detected via the AFM tip, thereby providing chemical information with nanometre resolution.
Examples of applications and contacts
Scanning electron microscopy (SEM)
- Characterisation of surface morphology and microstructures
- Particle measurement and shape analysis
- Quality control of coated surfaces
- Material testing of fracture surfaces and signs of wear
- Development of nanostructured materials
Transmission electron microscopy (STEM)
- Atomic structural analysis of nanomaterials
- Characterisation of interfaces and defects
- Phase distribution in nanostructures, chemical analysis at the nanoscale
Professor Tung Pham
Department of Textile Chemistry
Höchsterstraße 73, 6850 Dornbirn
+43 (5572) 28533
Email Website
Device: Scanning electron microscopy (SEM) at room temperature in a rough vacuum
Company: Hitachi
Model: TM4000Plus II TA
Researchinfrastructure Database
Analysis is possible for small sample quantities, provided that resources are available
Professor Oliver I. Strube
Department of Chemical Engineering
Innrain 80–82, 6020 Innsbruck
+43 (512) 507 55300
Email Website
Devices:
- Scanning electron microscope (SEM):
Compan/Model: Thermofisher/Phenom XL with EDX Detector - Scanning Electron and Scanning Transmission Electron Microscope (SEM and STEM)
Firma/Modell: Tescan/Clara with EDX-, EBSD-, STEM-Detector
Dr Nikolaus Weinberger
Department of Structural Engineering and Material Sciences
Technikerstraße 13, 6020 Innsbruck
+43 (512) 507 63548
Email Website
Devices: several Scanning Electron microscopes (SEM)
Comapny/Model:
- Oxford Instruments/AZtecLive Advanced mit Ultim Max 100 (with EDS Detektor)
- FEI/Quanta 3D 200 - Research Infrastructure Database
- Thermo Fisher/Axia ChemiSEM LoVAc - Research Infrastructure Database
Scanning tunnelling microscopy (STM) and scanning tunnelling spectroscopy (STS)
- Atomic resolution of conductive surfaces
- Investigation of surface reconstructions and defects
- Analysis of adsorption processes at the atomic level
- Determination of local electronic properties
Atomic force microscopy (AFM)
- Topographical characterisation with atomic resolution of non-conductive surfaces
- Investigation of biomolecules under physiological conditions
- Characterisation of 2D materials and thin films
Atomic force microscopy with IR coupling (AFM-IR)
- Investigation of degradation processes in materials
- Development of functional coatings
- Quality control in microelectronics
- Chemical mapping of polymer blends and composites
- Characterisation of membranes and cell structures
Professor Martin Beyer
Department of Ion Physics and Applied Physics
Technikerstraße 25, 6020 Innsbruck
+43 (512) 507 52680
Email Website
Gerät: Atomic Force Microscope (AFM)
Comapny: Bruker
Model:JPK Nanowizard 4
Research Infrastructure Database
Analysis of samples as part of collaborative projects (including biological samples)
Associate Professor Dr Laerte Patera
Department of Physical Chemistry
Innrain 52c, 6020 Innsbruck
+43 (512) 507 58100
Email Website
Devices -Scanning tunnelling microscopes (STM)
- Variable-temperature STM - Research Infrastructure Database
- STM: Nanosurf - Easyscan - internal description
Scanning tunneling/-atomic force microscopes (STM/AFM)
- Low-tempearture STM/AFM, Createc, LT-STM/AFM - Research Infrastructure Database
- STM/AFM, Infinity - Scienta Omicron
Details:
- Microscopy in ultra-high vacuum at low to room temperature (5–77–300 K)
- Scanning tunnelling microscope, scanning tunnelling spectroscopy (STM, STS)
- Atomic force microscope (non-contact mode, nc-AFM)
Professor Oliver I. Strube
Department of Chemical Engineering
Innrain 80–82, 6020 Innsbruck
+43 (512) 507 55300
Email Website
Device: Atomic Force Microscope with IR coupling (AFM-IR)
Company: Bruker
Model: nanoIR3
internal description - Research Infrastructure Database
additional devices and contacts
